Krone NIR Control dual with calibration model 14.3.1

DLG-APPROVED: "Ingredients in liquid cattle manure, liquid pig manure, mixed manure from cattle and pig manure and in liquid digestate"

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Test report 7273

KRONE NIR Control dual

The approval

A test mark „DLG-APPROVED for individual criteria“ is awarded for agricultural products which have successfully fulfilled a scope-reduced usability testing conducted by DLG according to independent and recognised evaluation criteria. The test is intended to highlight particular innovations and key criteria of the test object. The test may contain criteria from the DLG test scope for overall tests, or focus on other value-determining characteristics and properties of the test subject. The minimum requirements, test conditions and procedures as well as the evaluation bases of the test results will be specified in consultation with an expert group of DLG. They correspond to the recognised rules of technology, as well as scientific and agricultural knowledge and requirements. The successful testing is concluded with the publication of a test report, as well as the awarding of the test mark which is valid for five years from the date of awarding. 

The DLG test for “recision of NIR sensors for the determination of ingredients in passing liquid ­manure of animal origin and liquid digestate from cattle or pig manure with renewable raw materials“ was carried out on the NIR Control dual with calibration model 14.3.1 of Maschinenfabrik Bernard Krone GmbH & Co. KG.

The measurements for determining the contents of ingredients were carried out in in liquid cattle manure, in liquid pig manure, in liquid mixed manure from cattle and pig manure and in liquid digestate from cattle or pig manure with renewable raw materials. In each manure type, five different practice slurries were examined through the tested sensor for their levels of dry matter content (DM in weight %), total nitrogen (NTotal in kg/m³), ammonium nitrogen (NH4-N in kg/m³), phosphate (phosphorous pentoxide; P2O5 in kg/m³), and potassium oxide (K2O in kg/m³). During the measurements from each slurry samples were collected.

The taken samples were analyzed by a total of five different accredited specialized laboratories, preferably with wet-chemical methods. For each ingredient, the averages from the results of the laboratory analyses were calculated. For the evaluation, the differences between the value measured by the NIR Sensor and the mean value of the laboratories were determined as the relative measurement deviation. The precision of the sensor was examined at different flow rates too. 

Other criteria were not tested.

Assessment in brief

On the basis of the results obtained the mobile sensor Krone NIR Control dual with calibration model 14.3.1 is awarded the DLG test mark “DLG APPROVED in single criteria” in the measurement of ingredients in liquid manures for the parameters listed in the following table 1.

Table 1: Overview of results

DLG quality profile
Ingredient
Evaluation 1
Cattle manure 
Dry Matter (DM) 
Total nitrogen (NTotal)
Ammonium nitrogen (NH4­N)
Phosphorous Pentoxide (P2O5)
Potassium oxide (K2O)
Pig manure 
Dry Matter (DM) 
Total nitrogen (NTotal)
Ammonium nitrogen (NH4­N)
Phosphorous Pentoxide (P2O5)
Mixed manure from cattle and pig manure 
Dry Matter (DM) 
Total nitrogen (NTotal)
Phosphorous Pentoxide (P2O5)
Potassium oxide (K2O)
Liquid digestate from cattle or pig manure with renewable raw materials 
Dry Matter (DM) 
Total nitrogen (NTotal)
Ammonium nitrogen (NH4­N)
Phosphorous Pentoxide (P2O5)

1  Evaluation range: Requirements fulfilled () / not fulfilled  (X)

The product

Description and technical data

The Krone NIR Control dual measuring system is a NIR (NearInfraRed) measuring system developed for the com­positional analysis of organic substances, such as animal farm fertiliser and digestates.

The Krone NIR Control dual is integrated into the existing pipe system of the pumping station or the manure tank truck. To ensure error-free functionality of the sensor the installation positions specified by the manufacturer must be observed.

In addition, the manufacturer offers also an application for the determination of ingredients in passing feed if the system is attached to the spout of KRONE forage harvesters. For use in the forage harvester the Krone NIR Control dual has a DLG recognition at the dry mass determination in corn with the calibration model ‘Mais 08 V3.0.1’ (see DLG test report 7222).

Figure 2: Functional principle and system structure Krone NIR Control dual
Figure 2: Functional principle and system structure Krone NIR Control dual

The method

The aim of the DLG Test „ Precision of mobile sensors for the determination of ingredients in passing liquid manure of animal origin and liquid digestate“ is to examine the accuracies of mobile sensors in con­junction with appropriate calibration models in comparison to laboratory analysis with officially recognized methods. 

A major advantage of NIR measuring technology compared to the conventional methods for the determination of ingredients in liquid manures through sampling and laboratory analysis, consists in the immediate availabi­lity of measurement results, and in the permanent measurement of the ingredients along the complete manure volume. 

Figure 3: Schematic structure of the DLG measuring system
Figure 3: Schematic structure of the DLG measuring system

The test results in detail

The trials were conducted jointly with the Educational Center located at Triesdorf, Germany (Landwirtschaft­liche Lehranstalten LLA, Triesdorf). Flow rates from 6 m³/min to 9 m³/min were set during the measurements. The different flow rates showed no influence on the measured values of the sensor. In table 3 the individual results are given.

Based on the obtained results, the mobile Sensor Krone NIR Control dual with calibration model 14.3.1 is awarded the test mark „DLG-APPROVED in individual criteria“ for the measurement of:

  • Ingredients in liquid cattle manure: DM, NTotal, NH4-N, P2O5, K2O
  • Ingredients in liquid pig manure: DM, NTotal, NH4-N, P2O5
  • Ingredients in mixed manure from liquid cattle and liquid pig manure: DM, NTotal, P2O5, K2O
  • Ingredients in liquid digestate from cattle or pig manure with renewable raw materials: DM, NTotal, NH4-N, P2O5

Table 3: Individual results

Type designationKrone NIR Control dual
with calibration model 14.3.1
Evaluation *
Installation position (tilt)90° 
Installation positionhorizontal 6" pipe 
   
Cattle manure  
 DM in % by weight+
 NTotal in kg/m³o
 NH4-N in kg/m³o
 P2O5 in kg/m³o
 K2O in kg/m³+ +
Pig manure  
 DM in % by weight+ +
 NTotal in kg/m³o
 NH4-N in kg/m³o
 P2O5 in kg/m³o
 K2O in kg/m³
Mixed manure from cattle and pig manure  
 DM in % by weighto
 NTotal in kg/m³+ +
 NH4-N in kg/m³
 P2O5 in kg/m³o
 K2O in kg/m³+
Liquid digestate from cattle or pig manure with renewable raw materials  
 DM in % by weighto
 NTotal in kg/m³+
 NH4-N in kg/m³+
 P2O5 in kg/m³o
 K2O in kg/m³

DLG-assesment scheme:
+ + = passed, very good (4/5 value pairs within a manure type ≤ 10 % and no > 20 % rel. deviation)
+ = passed, good (4/5 value pairs within a manure type ≤ 15 % and no > 25 % rel. deviation)
o = passed (3/5 value pairs within a manure type ≤ 25 % and no > 35 % rel. deviation)
– = failed

Summary

The sensor NIR Control dual with calibration model 14.3.1 of Maschinenfabrik Bernard Krone GmbH & Co. KG fulfilled the requirements for DLG approval in the accuracy of measurement of dry matter (DM), total nitrogen (NTotal), and Phosphorous Pentoxide (P2O5) in liquid cattle and pig manure, in mixed manure from cattle and pig manure and in liquid digestate from cattle or pig manure with renewable raw materials.

In addition, the system meets the DLG requirements for ammonium nitrogen (NH4-N) in cattle and pig manure as well as liquid digestate from cattle or pig manure with renewable raw materials and for potassium oxide (K2O) in cattle manure such as mixed manure from cattle and pig manure.

A major advantage of NIR measuring technology compared to the conventional methods for the determination of ingredients in liquid manures through sampling and laboratory analysis, consists in the immediate availability of measurement results, and in the permanent measurement of the ingredients along the complete manure volume. 

Manufacturer and test implementation

Manufacturer and applicant

Maschinenfabrik Bernard Krone GmbH & Co. KG
Heinrich-Krone-Str. 10
48480 Spelle, Germany

Test implementation

Testing agency 
DLG TestService GmbH, Gross-Umstadt location, Germany
Landwirtschaftliche Lehranstalten, Triesdorf

The tests are conducted on behalf of DLG e.V. 

DLG test framework 
“Precision of NIR sensors for the determination of ingredients in passing liquid manure of animal origin and liquid digestate” (current as of 09/2020)

Department
Agricultural technology

Members of the competent 
DLG Test Commission “Fertilising Technology“
Dr. Horst Cielejewski, Chamber of Agriculture of North Rhine-Westphalia
Dr. Harm Drücker, Chamber of Agriculture of Lower Saxony
Prof. Nils Fölster, University of Osnabrück
Prof. Hans W. Griepentrog, University of Hohenheim
Dr. Fabian Lichti, State Institute of Agriculture Bavaria
Frank Reith (farmer), Groß-Umstadt
Sven Schneider (farmer and contractor), Brensbach
Peter Seeger (farmer), Otzberg

Division head 
Dr. Ulrich Rubenschuh*

Test engineer(s)
Dipl. Ing. agr. Georg Horst Schuchmann

*Author

Contact us

DLG TestService GmbH - Groß-Umstadt location • Max-Eyth-Weg 1 • 64823 Groß-Umstadt • Tel: +49 69 24 788-600 • tech@DLG.org